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Authors: E.S. Mikhailova, S.R. Khairulin, A.V. Salnikov, Kuznetsov , AS. Chichkan, V.V. Chesnokov, Podyacheva , Z.R. Ismagilov

Title of the article: Development and construction of the installation for catalytic synthesis of carbon nanomaterials

Year: 2017, Issue: 4, Pages: 135-146

Branch of knowledge: Chemical technology

Index UDK: 54.053

DOI: 10.26730/1999-4125-2017-4-135-146

Abstract: A laboratory installation for the catalytic synthesis of nitrogen-containing CNM with two parallel reactors with a capacity of up to 100 grams of СNM per hour was developed and constructed. The installation allows us to study the synthesis of carbon nanomaterials both in a reactor with a vibrating catalyst bed and in a flow tube reactor using both gaseous (ammonia, ammonia-containing gas mixtures) and liquid (acetonitrile, pyridine, dimethylformamide) nitrogen-containing compounds. The installation allows variation of the synthesis conditions of the CNM within a wide range of parameters (the composition of the initial reaction mixture, the feed rate of the initial reaction mixture, the reaction temperature).

Key words: сarbon nanomaterials nitrogen-containing carbon nanomaterials synthesis

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